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The reduction of DHLA-Ala- Au 3+ Cl 4 complexes was complete to form DHLA-Ala@AuNPs in 2 min because DHLA-Ala ligand slightly undergoes deprotonation

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B-Max and Z-Max were synthesized by SPPS with bis-alkylated, terminal olefin-containing S 5 amino acid incorporated at strategic i and i + 4 positions

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