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The MS settings were as follows: scan range(m/z) 70-800, resolution 500,000 at m/z 200, RF lens (%) 30, sheath gas flow rate 50 arbitrary units (Arb), auxiliary gas flow at 10 Arb, sweep gas flow at 1 Arb, ion transfer tube temperature 325 C, vaporizer temperature 350 C, and negative ion voltage 2 500 V